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A Remarkable Synergic Effect of Polymer-anchored Bimetallic Palladium-Ruthenium Catalysts in the Selective Hydrogenation of p-Chloronitrobenzene

A synergic effect of the polymer-anchored bimetallic palladium-ruthenium catalysts can lead to a remarkable increase in the selectivity for p-chloroaniline in the selective hydrogenation of p-chloronitrobenzene under atmospheric pressure and in the presence of a small amount of base.

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Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Effective octadecylamine system for nanocrystal synthesis

New chemical reactions and synthetic systems are of key importance for materials fabrication. In this work, we reported a facile and effective octadecylamine (ODA) synthetic system for various nanocrystals including metals, mixed metal oxides, metal/metal oxide heterostructured nanocrystals, intermetallics, and alloys. We found that the products were mainly determined by metal ions used in our synthetic system: noble metal ions led to the formation of metals; two kinds of nonnoble metal ions led to the formation of mixed metal oxides; silver ions and non-noble metal ions led to the formation of metal/metal oxide heterostructured nanocrystals; non-noble metal ions and noble metal (excluding Ag) ions led to the formation of intermetallics and alloys. The difference was attributed to different ability to attract electrons from ODA solvent among these metal ions. This effective system provides a general strategy for various nanocrystals which would find potential applications in many significant fields.

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Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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The reactant in an enzyme-catalyzed reaction is called a substrate. Enzyme inhibitors cause a decrease in the reaction rate of an enzyme-catalyzed reaction.I hope my blog about 10049-08-8 is helpful to your research., Computed Properties of Cl3Ru

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Methanol electro-oxidation at Ptx Ru(1-x)O y electrodes – An in situ FTIR study

In this work we investigated the nature of the intermediates adsorbed during the electrooxidation of methanol on PtxRu (1-x)Oy electrodes, where 0.5 < x < 0.9, prepared by the decomposition of polymeric precursors. Thin layer electrodes with different compositions were prepared directly on a gold substrate by thermal decomposition of ethylene glycol - citric acid solutions containing the precursor salts at 400C. In situ IR reflectance spectra were obtained using the SPAIRS (single potential alteration infrared reflectance spectroscopy) and SNIFTIRS (subtractively normalized interfacial Fourier transform IR reflectance spectroscopy) techniques. For all the investigated compositions, the SNIFTIRS and SPAIRS spectra displayed three main bands, which were attributed to CO species in the linear (COL) and bridged (COB) forms adsorbed over Pt and linearly adsorbed over Ru. Formation of CO2 carbonyl species was also detected. The spectra features were analyzed in terms of the applied potential and they were compared with those reported for Pt-Ru electrodes prepared by other methods. The reactant in an enzyme-catalyzed reaction is called a substrate. Enzyme inhibitors cause a decrease in the reaction rate of an enzyme-catalyzed reaction.I hope my blog about 10049-08-8 is helpful to your research., Computed Properties of Cl3Ru

Reference£º
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Mild and selective Ru-catalyzed formylation and Fe-catalyzed acylation of free (N-H) indoles using anilines as the carbonyl source

C3-selective formylation and acylation of free (N-H) indoles under mild conditions can be achieved by using Ru- and Fe-catalyzed oxidative coupling of free (N-H) indoles with anilines, respectively. Both processes are operationally simple, compatible with a variety of functional groups and generally provide the desired products in good yields. 13C-labeling experiments unambiguously established that the carbonylic carbon in the formylation products originated from methyl group of N-methyl aniline.

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Reference£º
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Improved capacity and rate capability of Ru-doped and carbon-coated Li 4Ti5O12 anode material

Pure Li4Ti5O12, modified Li 4Ti5O12/C, Li4Ru 0.01Ti4.99O12 and Li4Ru 0.01Ti4.99O12/C were successfully prepared by a modified solid-state method and its electrochemical properties were investigated. From the XRD patterns, the added sugar or doped Ru did not affect the spinel structure. The results of electrochemical properties revealed that Li4Ru0.01Ti4.99O12/C showed 120 and 110 mAh/g at 5 and 10 C rate after 100 charge/discharge cycles. Li 4Ru0.01Ti4.99O12/C exhibited the best rate capability and the highest capacity at 5 and 10 C charge/discharge rate owing to the increase of electronic conductivity and the reduction of interface resistance between particles of Li4Ti5O 12.It is expected that the Li4Ru0.01Ti 4.99O12/C will be a promising anode material to be used in high-rate lithium ion battery.

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Reference£º
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Carbonate selective Ca2Ru2O7-y pyrochlore enabling room temperature carbonate fuel cells: I. Synthesis and physical characterization

Synthesis of a carbonate selective Ca2Ru2O 7-y catalyst was investigated using solid-state and hydrothermal routes. The resulting materials were physically characterized by x-ray diffraction, BET gas adsorption, scanning electron microscopy and temperature programmed desorption. The solid-state reaction of precursor oxides, CaO and RuO2, led to the formation of a perovskite phase. A hydrothermal route using O2 as an oxidizing agent yielded a mostly amorphous phase primarily comprised of unreacted precursor. The use of low concentration KMnO4 (10 mM) as a replacement for O2 in the hydrothermal synthesis, in combination with high pH (?14) and moderate temperature (200C), yielded a highly crystalline, thermally stable Ca 2Ru2O7-y pyrochlore. The increase in crystallinity was attributed to the ability of permanganate to maintain ruthenium in the +5 oxidation state required for formation of the pyrochlore phase. Micron-sized primary particles with a high density of ? 50 nm surface nanocrystallites were obtained. The presence of the nanocrystallites gave the pyrochlore a high surface area, 174 m2/g. The pyrochlore showed preferential surface adsorption of CO2 compared to H2O, making it a feasible candidate for a carbonate selective catalyst. This preferential adsorption was attributed to the use of calcium, an alkaline earth metal, which gave the pyrochlore a high surface basicity.

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Reference£º
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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(+)-Saxitoxin: A first and second generation stereoselective synthesis

A stereoselective synthesis of the bis-guanidinium toxin (+)-saxitoxin (STX), the agent infamously associated with red tides and paralytic shellfish poisoning, is described. Our approach to this unique natural product advances through an unusual nine-membered ring guanidine intermediate 39 en route to the tricyclic skeleton that defines STX. The effectiveness of this strategy is notable, as only four steps are needed to transform 39 into the target molecule, including a four-electron alkene oxidation catalyzed by OsCl3. Construction of the critical monocyclic guanidine has been achieved through two channels, the first of which makes use of Rh-catalyzed C-H amination and highlights a novel class of heterocyclic N,O-acetals as iminium ion equivalents for crafting functionalized amines. A second route to 39 relies on a stereoselective acetylide dianion addition to a serine-based nitrone, thereby facilitating the preparation of STX in just 14 linear steps from commercial material.

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Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Rh-catalyzed one-pot and practical transformation of aldoximes to amides

Wilkinson’s complex has been found to catalyze the one-pot transformation of aldoximes to the corresponding amides with high selectivity and efficiency under essentially neutral conditions.

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Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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In situ XANES studies of electrodeposited nickel oxide films with metal additives for the electro-oxidation of ethanol

Electrodeposited nickel oxide electrodes with additives such as sodium, cobalt, ruthenium, and their combination were evaluated as the anode materials for the electro-oxidation of ethanol using in situ x-ray absorption near edge structure (XANES). Electro-chemical chemical properties of the electrodes were studied by monitoring oxidation states of metal oxides during oxidation of electrodes themselves, as well as during oxidation of ethanol, in alkaline media. The Ni-Co-Ru electrode showed the best performance with increased anodic peak currents and lower overvoltages for electrochemical oxidation of ethanol. Analysis of the XANES data for the Ni and Co K-edges of these composite electrodes revealed that both Ni and Co are in the Ni3+-Ni4+ and Co3+ -Co4+ mixed states, respectively, depending on applied potentials. The presence of cobalt and/or ruthenium in nickel oxide films enhanced the electrode performances for ethanol oxidation due to generation of highly oxidized states of cobalt and ruthenium via electrogenerated nickel oxides.

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Reference£º
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Birefringence in guest-host Ru-containing chromophore induced by acoustic field

We have observed firstly a difference in birefringence caused by left- and right-handled circularly polarized acoustical fields for organometallic racemic tris(phenanthroline)ruthenium(II) dichloride chromophore incorporated within the polymethacrylate polymer. Within the acoustic power densities 1.2-2.2 W/cm 2, this difference substantially increases up to the birefringence value of about 0.003. After the switching off of the acoustical field, the induced birefringence disappears after 14 s birefringence decay kinetics after switching off the acoustic field consists from two parts (at 8 and 14 s).

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Reference£º
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI